|
|
Preparation of high-valueable gypsum binder
Hájková, Iveta ; Gazdič,, Dominik (referee) ; Fridrichová, Marcela (advisor)
This work is oriented on the preparation of high-voluable sulphate binder based on gypsum waste. One of the potential mineral resources in Moravia is Pregips chemical gypsum, produced by Precheza. This is the raw material, which is characterized by high purity, high quality and is economically acceptable. Beta burned gypsum plaster from this, however, need to modify due to suppression of the high needs of water mixing, which is determined by its morphology. The need for mixing water has a large impact on the strength of gypsum binders. Therefore it is necessary to find a suitable additive, which would reduce the coefficient of water in the preparation of porridge normal consistency.
|
|
|
Preparation of modified tricalcium aluminate phases and study of their hydratation processes
Vávrová, Alžběta ; Koplík, Jan (referee) ; Másilko, Jiří (advisor)
This diploma thesis deals with the preparation of modified tricalcium aluminate phases using sodium ions, and the study of their hydration processes and products. The X-ray diffraction analysis, isothermal calorimetry, laser diffraction, and scanning electron microscopy with energy dispersion analysis were used to solve this task. The preparation of modified tricalcium aluminate phases using high temperature methods has been described in the experimental section. Furthermore, the X-ray diffraction analysis was used to determine the purity of the prepared phases and the scanning electron microscopy with energy dispersion analysis was used to define the volume of sodium. Laser diffraction was used to measure a particle size distribution in the individual phases. Subsequently, hydration of the pure phases was performed in an isothermal calorimeter. It was followed by hydration of phases in the presence of different gypsum content and then in the presence of saturated portlandite solution. Hydration of some samples was stopped in order to better understand the hydration process. Hydration products were studied by X-ray diffraction analysis. The obtained results were compared with each other and the influence of sodium ions on both the structure of the prepared phases and the course of hydration and its products has been discussed. The effect of adding different volumes of gypsum and portlandite on the course of hydration of the individual phases was also compared.
|
|
|
Methods of excitation of binders based on anhydrite
Sedlák, Michal ; Dvořák, Karel (referee) ; Gazdič, Dominik (advisor)
The bachelor thesis deals with the internal excitation of anhydrite-based mortars. In the theoretical part, the general theory of sulphate binders, the formation of gypsum binders and their resulting products during firing are described. The theoretical part also describes the anhydrite mortars, their hydration process and collects the existing research on anhydrite excitation in the world, where, among other things, it deals with the further usability of the resulting gypsum by-products. The experimental part focuses on the internal excitation of anhydrite, which is based on the existing research at the THD Institute. The work builds on previous studies that also dealt with internal excitation research. It includes an experiment performed to optimize the thermal regime in the form of increased isothermal endurance with subsequent evaluation by XRD analysis.
|
|
| |
|
|
Study of Hydration of Anhydrite Binders
Duda, Štěpán ; Smetanová,, Lenka (referee) ; Gazdič, Dominik (advisor)
Presented bachelor thesis deals with the study of hydration of anhydrite binders. This thesis is primary focused on testing the various hydration exciters of anhydrite and subsequent monitoring of the hydration process by the XRD analysis and also builts on previous research in this area at the institute of THD. Conceptually is this work divided into two parts. The first part deals with the general theory of sulphate binders. The second part is devoted to the partical testing of the various hydration exciters and their subsequent comparsion.
|
|
|
Comparison of microstructure of standard and modified fly ash autoclaved aerated concrete
Fleischhacker, Ján ; Kulísek, Karel (referee) ; Drochytka, Rostislav (advisor)
Nowadays, the amount of produced fly ash and fluidized ash is huge, so it is important to find ways of its proper use.Significant influence in field of fly ash consumption is production of autoclaved aerated concrete. Most important factor in production is properties of raw materials such as mineralogical and chemical composition. The study of raw materials is important to understand the mechanism of hydratation, tobermorite formation and mineralogy of final product. In present study, we investigate influence of raw materials to mineralogy of autoclaved aerated concrete, significantly to influence of fluidized ash on quality of autoclaved aerated concrete. Closure of study is design of the methodology, specialized in field of bachelor’s thesis study.
|
|
| |
|
|
Methods of Excitation of Sulphate Binder Based on Anhydrite
Adameková, Paulína ; Vavrušková,, Lenka (referee) ; Gazdič, Dominik (advisor)
The presented bachelor thesis is focused on excitation of a sulfate binder based on anhydrite. The thesis is conceptually divided in a theoretical and experimental part. The theoretical part is devoted to the general theory of sulphate binders and anhydrite mortars, at the same time, there is brought view on process of production of historical gypsum binders as well as the current use of anhydrides. In theoretical part of the thesis, there is included study, which is focused on previous research in presented problematics at the THD institution. In the experimental part of the thesis, which is primarily focused on the method of internal excitement, there is elaborated design and mineralogical analysis of input feedstocks as well as the internal waking process itself with subsequent qualitative evaluation using XRD and REM analysis.
|
|
| |
|
|
Research on high-performance preparation sulphate binders
Haluska, Lukáš ; Novák, Jan (referee) ; Fridrichová, Marcela (advisor)
The thesis is focused on preparation of high – valuable gypsum binder. Following the current state was performed design of sulphate premix, which will be used as binder of plaster mixture, leveling and corrective cement. Teoretical part of task is dedicated to a existing research of sulfate binders with an emphasis on technological properties of beta-gypsum. In Experimental part of task is designed premix and assessment basic technological properties.
|
guest ::
